I noticed that slightly touching the mount of the first mirror on the HeNe probe path makes the beam deflect a lot. So I changed it with a more rigid mirror mount.
I also wanted to clean the mirror (Thorlabs 1/2" Protected silver mirror PF05-03-P01), but I broke it, so I replaced it with a Newport 5103 General Purpose Silver Coated Mirror that I found in Tama.
Then I aligned the HeNe probe using the pinhole. The beam passes through the following positions of the pinhole:
z | y | |
start | 15 | 122.373 |
default | 38.85 | 120.823 |
end | 115 | 115.873 |
I noticed that the reflection of the first lens on the IU was going up to the chopper. This is very likely to generate noise in phase, so I tilted the lens of the IU.
I also noticed another reflection from the sample that is going to the chopper. I can't tilt the sample, so I solved it putting a simple aperture near the chopper. See picture.
I used the surface reference to align the pump and maximize the AC signal.
I used the new power meter for the pump:
pump power: 74mW , chopper on: 37mW, with surf ref sample: 27mW
I moved the imaging unit to find the maximum of the signal on the surf ref.
IU pos | AC | DC | AC/DC |
60mm | 0.26 | 4 | 0.065 |
65mm | 0.32 | 4.2 | 0.076 |
70mm | 0.36 | 4.4 | 0.082 |
75mm | 0.51 | 4.75 | 0.107 |
The maximum is not in the range of the IU stage. Probably because tilting the lens to move the probe reflection from the chopper, I missed the focus of the IU telescope.
Therefore I started again the IU alignment. I put the IU stage at 60mm. I found the sharp image of the blade. I looked for the maximum of absorption signal again:
IU pos | AC | DC | AC/DC |
60mm | 0.59 | 6.4 | 0.092 |
65mm | 0.64 | 6.4 | 0.1 |
70mm | 0.72 | 6.4 | 0.112 |
75mm | 0.6 | 6.4 | 0.094 |
So I put the IU at 70mm.
I made a scan of the surf reference.
I noticed that the DC is not linear with the power of the probe. I measured 6.4V for 1.71mW, and 6.5V for 2.58mW. Then I replaced the LDS9 power supply with the 12V battery and the 2.58mW gave 9V of DC. So I decided to keep the DC below 6V with a OD wheel, and continue using the LDS9 power supply.
After putting the wheel, I missed the alignment pump/probe, so I used again the pinhole to center the probe.
Then I made a scan of the surf reference again.
And a scan of the bulk reference. The transmitted power is 20mW (of 37mW incident)